光譜儀在使用中難免會出現這樣那樣的問題,而作為儀器使用人員,往往缺少必要的儀器維護知識,我們總結了一些直讀光譜儀使用中常見的簡單問題,希望能對企業用戶有所幫助
In the use of spectrometer will inevitably have such problems as instruments often lack the necessary personnel, equipment maintenance knowledge, we summarize some common problems of simple spectrometer use, hope to help enterprise users
故障一:新儀器電腦出現死機,程序錯誤、黑屏、分析軟件的 START狀態不對有時變為黃色不動,有時雖然動但是變為紅色。
Fault: a new instrument computer crashes, program error, black, analysis of START software into the wrong state sometimes yellow does not move, though sometimes but turn red.
處理辦法:此為通訊線接觸不良,重新連接即可。
Processing method: This is bad communication lines, re connect to.
故障二:光譜儀排氣不暢故障,氬氣排氣管路堵塞,火花室下部的彎
Fault two: spectrometer exhaust failure, argon exhaust pipe blockage, the lower part of the spark chamber
頭內有異物,氬氣過濾器入口端有異物。
There are foreign bodies in the head, and the inlet of the argon filter has foreign bodies.
處理辦法:更換排氣管,要更換透明的塑料管,并定期對排氣管路進行吹掃。
Treatment methods: replace the exhaust pipe, to replace the transparent plastic pipe, and the exhaust pipe on the purge.
故障三:溫度偏高故障
Fault three: high temperature failure
處理辦法:檢查儀器后蓋風扇是否轉動,轉動是否靈活。
Treatment method: check whether the instrument back cover fan rotation, rotation is flexible.
故障四:真空泵不自動啟動故障,
Fault four: vacuum pump does not automatically start failure,
處理辦法:先看泵油溫度是否較低,重新斷電后,手動啟動真空泵,有時需停頓一下,再試。
Treatment methods: first look at the pump oil temperature is low, after the power outage, manually start the vacuum pump, sometimes need to pause, try again.
故障五:光譜儀 P、S 穩定性不好,檢查真空泵是否被誤關掉,真空光路鏡片是否需要清洗,一個維護不好的光路會導致錯誤的重現性和
Fault five: spectrometer P, S stability is not good, check whether the vacuum pump is turned off, the vacuum optical path lens need to be cleaned, a poor maintenance of the optical path will lead to false reproducibility and
分析結果。
Analysis result.
處理辦法:檢查真空泵及清洗鏡片
Treatment methods: check the vacuum pump and cleaning lens
故障六:真空值下降快故障
Fault six: vacuum value decreased fast failure
處理辦法:看真空值曲線是否平緩,否則,有漏氣的地方,檢查真空室真空蓋密封性,更換密封圈或對角緊固螺絲。
Treatment method: see the vacuum value curve is gentle, otherwise, there is a leak, check the vacuum chamber vacuum seal, replace the sealing ring or diagonal fastening screws.
故障七:光譜儀光強值下降
Fault seven: spectral light intensity decreased
原因分析:
Reason analysis:
1、透鏡臟
1, lens dirty
2、入射狹縫污染
2, incident slit pollution
3、光纖老化
3, optical fiber aging
處理辦法:擦拭透鏡,清理狹縫,更換光纖。
Solution: wipe the lens, clean the slit, replace the optical fiber.
經驗總結:光譜儀用久了,激發臺會因點打的太多了,出現放電漏氣現象,導致光強上不去,需要經常清理激發臺板及火花室。
Experience: spectrometer with a long time, because Taiwan will be excited to play too much, resulting in leakage discharge occurs, the intensity can not go up, need to clean up the table and stimulate the spark chamber.
故障八:數據不穩定
Fault eight: Data instability
處理方法: 清洗鏡片后重新做標準化,儀器鏡片的污染會導致數據測試的結果不穩定,長時間沒有做儀器的曲線校準也會導致數據測試
Processing method: after cleaning the lens to do standardization, instrument lens pollution will lead to the result of data testing is not stable, long time did not do the calibration of the instrument curve will lead to data testing
穩定性不好。
Poor stability.